Supercritical Drying Experimental Device

Supercritical Drying Experimental Device


The drying process of the gel is crucial for the preparation of aerogels. Traditional methods lead to coarsening of the base particles, a significant decrease in specific surface area, and a large reduction in porosity. However, supercritical fluid drying technology, due to the supercritical fluid's combined gas-liquid properties, absence of surface tension, and additional pressure, can prevent gel structure collapse and shrinkage, maintaining the network framework structure. This results in ultrafine aerogels with high specific surface area, uniform particle size distribution, and large pore volume. Aerogels, as porous nanomaterials with high specific surface area and low bulk density, have broad application prospects in aerospace, catalysis, environmental protection, and other fields due to their unique nanostructure. Their common preparation method, the sol-gel process, includes three stages: sol preparation, gel preparation, and gel drying.
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Convenient and easy to use

 

Graphical user interface

Easy and understandable operation


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Reliable and stable

 

High accuracy, high stability

 

 


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Personalized customization

 

Can be customized according to needs

Enhance device configuration

     

Application Fields

 

 

Application Functions

Product Parameters

Parameter Indicators

Drying Kettle

Room temperature to 80℃, heated by water bath; radial seal on plug

Volume 10L, maximum working pressure 30MPa, with removable material basket

Separation Kettle Room temperature to 80℃, water bath heating, maximum working pressure 16MPa
CO 2 High-Pressure Pump Flow rate 100L/h, maximum discharge pressure 30MPa, frequency control for flow, equipped with accumulator to suppress pressure fluctuations
Cooling System Temperature control -5℃ to room temperature, equipped with external circulation pump
Filter Filters carbon dioxide or impurities in the pipeline to protect the high-pressure pump
Dryer Used to dry moisture carried by carbon dioxide, can be heated to 100℃ to remove moisture from the desiccant
Heat Exchange System

Extraction temperature control range adjustable from room temperature to 85℃, water bath heating;

Separation temperature control range adjustable from room temperature to 85℃, water bath heating

Metal Rotor Flow Meter 0~100L/h, 10MPa, used for CO2 flow measurement

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